Structures by: Zhang Z. M.
Total: 89
C26H25F3NOS
C26H25F3NOS
Organic Chemistry Frontiers (2017) 4, 9 1772
a=23.660(2)Å b=10.2673(10)Å c=10.5398(10)Å
α=90.00° β=90.00° γ=90.00°
C27H23ClF3NO3
C27H23ClF3NO3
Organic Chemistry Frontiers (2017) 4, 9 1772
a=8.5817(2)Å b=10.4128(3)Å c=27.6259(7)Å
α=90.00° β=90.00° γ=90.00°
C15H16F3NO2S
C15H16F3NO2S
Organic Chemistry Frontiers (2017) 4, 9 1772
a=6.2282(2)Å b=7.0351(2)Å c=36.2461(13)Å
α=90.00° β=90.00° γ=90.00°
C23H20Br2N2O2
C23H20Br2N2O2
Organic Chemistry Frontiers (2016) 3, 6 759
a=13.4028(8)Å b=11.2931(6)Å c=14.0439(8)Å
α=90.00° β=91.990(2)° γ=90.00°
C36H56AuClNOPS
C36H56AuClNOPS
Organic Chemistry Frontiers (2016) 3, 6 759
a=12.5457(6)Å b=22.3820(10)Å c=12.6621(5)Å
α=90.00° β=92.0520(10)° γ=90.00°
C48H191Co5N40O126Sb9W24
C48H191Co5N40O126Sb9W24
Chem. Sci. (2016) 7, 7 4220
a=27.14990(10)Å b=27.14990(10)Å c=27.14990(10)Å
α=90.00° β=90.00° γ=90.00°
C60H235ClCo4N49O133Sb9W24
C60H235ClCo4N49O133Sb9W24
Chem. Sci. (2016) 7, 7 4220
a=21.9241(13)Å b=26.1040(15)Å c=42.1665(19)Å
α=90.00° β=119.618(2)° γ=90.00°
C15H16N4O4S
C15H16N4O4S
Journal of agricultural and food chemistry (2017)
a=7.9986(16)Å b=10.370(2)Å c=11.701(2)Å
α=106.83(3)° β=106.02(3)° γ=104.49(3)°
C21H20BrClF3NO3
C21H20BrClF3NO3
Chem. Commun. (2017)
a=7.9928(7)Å b=10.3771(9)Å c=12.8507(11)Å
α=90.00° β=98.625(2)° γ=90.00°
C21H16BrClF3NO4
C21H16BrClF3NO4
Chem. Commun. (2017)
a=18.4648(12)Å b=10.5267(7)Å c=22.6707(15)Å
α=90.00° β=104.961(2)° γ=90.00°
C25H104N24Ni5O73P2W19
C25H104N24Ni5O73P2W19
RSC Advances (2013) 3, 43 20829
a=21.4954(13)Å b=21.4954(13)Å c=21.4954(13)Å
α=90.00° β=90.00° γ=90.00°
C36H28
C36H28
RSC Advances (2018) 8, 27 15173
a=8.5141(17)Å b=17.426(4)Å c=17.000(3)Å
α=90.00° β=97.44(3)° γ=90.00°
C56H44
C56H44
RSC Advances (2018) 8, 27 15173
a=8.1823(16)Å b=12.694(3)Å c=19.994(4)Å
α=90.14(3)° β=93.52(3)° γ=101.80(3)°
C30H42LiN3O13V
C30H42LiN3O13V
CrystEngComm (2013) 15, 3 459
a=18.079(4)Å b=16.435(3)Å c=11.603(2)Å
α=90.00° β=90.00° γ=90.00°
C16.5H17.5N1.5NaO9.5V
C16.5H17.5N1.5NaO9.5V
CrystEngComm (2013) 15, 3 459
a=20.463(4)Å b=20.463(4)Å c=27.880(7)Å
α=90.00° β=90.00° γ=120.00°
C20H104AsCu5N20Nb8O56V8
C20H104AsCu5N20Nb8O56V8
RSC Adv. (2015)
a=12.907(3)Å b=14.153(3)Å c=14.277(3)Å
α=89.48(3)° β=80.34(3)° γ=63.81(3)°
C20H98AsCu5N20Nb9O53V7
C20H98AsCu5N20Nb9O53V7
RSC Adv. (2015)
a=25.852(5)Å b=27.121(5)Å c=24.729(5)Å
α=90.00° β=109.49(3)° γ=90.00°
C36H28.5N3.5
C36H28.5N3.5
RSC Adv. (2016)
a=27.518(12)Å b=9.894(4)Å c=45.122(19)Å
α=90.00° β=106.22(2)° γ=90.00°
C35H28N21.5(CH3OH)
C35H28N21.5(CH3OH)
RSC Adv. (2016)
a=7.275(2)Å b=9.280(3)Å c=23.640(7)Å
α=83.829(6)° β=88.466(6)° γ=79.361(6)°
Cu2Dy2H50K3Na5O91Sb2W18
Cu2Dy2H50K3Na5O91Sb2W18
RSC Adv. (2015)
a=12.101(2)Å b=18.624(4)Å c=22.956(5)Å
α=104.53(3)° β=97.88(3)° γ=107.70(3)°
C28H24Ag9Mo12N16O41P
C28H24Ag9Mo12N16O41P
RSC Adv. (2016)
a=18.0182(7)Å b=18.0182(7)Å c=19.6454(15)Å
α=90.00° β=90.00° γ=90.00°
C15H13Cl2N3O4S
C15H13Cl2N3O4S
RSC Adv. (2017) 7, 6 3145
a=11.3908(12)Å b=8.3911(7)Å c=18.9319(19)Å
α=90.00° β=106.049(2)° γ=90.00°
C33H24N2O3
C33H24N2O3
RSC Adv. (2016)
a=5.616(3)Å b=9.350(4)Å c=25.070(10)Å
α=88.325(10)° β=87.442(9)° γ=83.160(9)°
2(NiO40PW11),5(C30H24N6Ni),1.08(H2O)
2(NiO40PW11),5(C30H24N6Ni),1.08(H2O)
RSC Adv. (2016)
a=28.977(3)Å b=16.7308(17)Å c=44.363(4)Å
α=90° β=97.407(2)° γ=90°
C20H16BN4NiO41W12,1.5(C30H24N6Ni)
C20H16BN4NiO41W12,1.5(C30H24N6Ni)
RSC Adv. (2016)
a=46.643(3)Å b=14.3057(8)Å c=25.9696(14)Å
α=90° β=90.006(2)° γ=90°
C20H16GeN4NiO41W12,1.5(C30H24N6Ni)
C20H16GeN4NiO41W12,1.5(C30H24N6Ni)
RSC Adv. (2016)
a=46.756(9)Å b=14.374(3)Å c=26.151(5)Å
α=90° β=90.35(3)° γ=90°
C12H152Dy6Fe6K9N12Na15O274Si6W60
C12H152Dy6Fe6K9N12Na15O274Si6W60
Dalton transactions (Cambridge, England : 2003) (2011) 40, 24 6475-6479
a=29.171(4)Å b=29.171(4)Å c=33.538(7)Å
α=90.00° β=90.00° γ=120.00°
C6H134Fe6K13N6Na17O280Si6Tb6W60
C6H134Fe6K13N6Na17O280Si6Tb6W60
Dalton transactions (Cambridge, England : 2003) (2011) 40, 24 6475-6479
a=20.788(11)Å b=35.596(17)Å c=38.39(2)Å
α=90.00° β=92.015(9)° γ=90.00°
C48H64Cu5Mo7N24O32
C48H64Cu5Mo7N24O32
Dalton transactions (Cambridge, England : 2003) (2012) 41, 14 4084-4090
a=10.357(2)Å b=12.884(3)Å c=15.307(3)Å
α=112.97(3)° β=98.94(3)° γ=101.66(3)°
C36H36Cu4Mo8N18O26
C36H36Cu4Mo8N18O26
Dalton transactions (Cambridge, England : 2003) (2012) 41, 14 4084-4090
a=12.469(3)Å b=13.905(3)Å c=18.135(4)Å
α=88.61(3)° β=70.12(3)° γ=73.73(3)°
C60H60Cu3Mo8N30O26
C60H60Cu3Mo8N30O26
Dalton transactions (Cambridge, England : 2003) (2012) 41, 14 4084-4090
a=12.583(3)Å b=13.642(3)Å c=14.263(3)Å
α=105.78(3)° β=114.65(3)° γ=101.16(3)°
C20H116Cu5N20Na6Nb12O56
C20H116Cu5N20Na6Nb12O56
Dalton transactions (Cambridge, England : 2003) (2013) 42, 16 5812-5817
a=13.092(3)Å b=20.171(4)Å c=17.283(4)Å
α=90.00° β=100.25(3)° γ=90.00°
C20H194Cu5Ge8N20Na10Nb32O163
C20H194Cu5Ge8N20Na10Nb32O163
Dalton transactions (Cambridge, England : 2003) (2013) 42, 16 5812-5817
a=15.104(3)Å b=25.920(5)Å c=30.280(6)Å
α=90.00° β=90.00° γ=90.00°
C42H46N12NiO41VW12
C42H46N12NiO41VW12
Dalton transactions (Cambridge, England : 2003) (2013) 42, 47 16602-16607
a=22.000(4)Å b=15.000(3)Å c=24.000(5)Å
α=90.00° β=90.00° γ=90.00°
C42H48CoN12O42VW12
C42H48CoN12O42VW12
Dalton transactions (Cambridge, England : 2003) (2013) 42, 47 16602-16607
a=22.024(4)Å b=15.065(3)Å c=24.120(5)Å
α=90.00° β=90.00° γ=90.00°
C7H22Cl2DyNO9
C7H22Cl2DyNO9
Dalton transactions (Cambridge, England : 2003) (2013) 42, 36 12853-12856
a=9.118(2)Å b=15.223(4)Å c=12.154(3)Å
α=90.00° β=109.432(5)° γ=90.00°
C18H107K3Mn3N3Nd6O172S2V39
C18H107K3Mn3N3Nd6O172S2V39
Dalton transactions (Cambridge, England : 2003) (2013) 42, 40 14445-14453
a=24.603(3)Å b=24.603(3)Å c=17.343(3)Å
α=90.00° β=90.00° γ=120.00°
C18H133K3La6Mn3N3O185S2V39
C18H133K3La6Mn3N3O185S2V39
Dalton transactions (Cambridge, England : 2003) (2013) 42, 40 14445-14453
a=24.559(3)Å b=24.559(3)Å c=17.082(2)Å
α=90.00° β=90.00° γ=120.00°
C18H109.5Ce6K1.5Mn3N3O172.5S2V39
C18H109.5Ce6K1.5Mn3N3O172.5S2V39
Dalton transactions (Cambridge, England : 2003) (2013) 42, 40 14445-14453
a=24.707(4)Å b=24.707(4)Å c=17.215(3)Å
α=90.00° β=90.00° γ=120.00°
H184K7Mn2Na15O243P6W41
H184K7Mn2Na15O243P6W41
Chemical communications (Cambridge, England) (2008) 14 1650-1652
a=19.481(4)Å b=22.414(5)Å c=29.869(6)Å
α=70.31(3)° β=72.36(3)° γ=71.26(3)°
Cu3H126K6Na14O214P6W41
Cu3H126K6Na14O214P6W41
Chemical communications (Cambridge, England) (2008) 14 1650-1652
a=19.186(4)Å b=21.040(4)Å c=26.248(5)Å
α=76.76(3)° β=82.43(3)° γ=73.42(3)°
H168K3Li5.5Na10Ni3.75O235P6W41
H168K3Li5.5Na10Ni3.75O235P6W41
Chemical communications (Cambridge, England) (2008) 14 1650-1652
a=19.187(4)Å b=20.947(4)Å c=28.482(6)Å
α=75.34(3)° β=79.86(3)° γ=73.54(3)°
C28H18Cu2N6
C28H18Cu2N6
CrystEngComm (2010) 12, 12 4378
a=23.631(3)Å b=4.8043(7)Å c=23.560(3)Å
α=90.00° β=116.741(2)° γ=90.00°
C28H21Br2Cu2N5
C28H21Br2Cu2N5
CrystEngComm (2010) 12, 12 4378
a=13.1150(19)Å b=22.273(3)Å c=10.6802(15)Å
α=90.00° β=118.973(2)° γ=90.00°
C52H40Cu10I10N8O2
C52H40Cu10I10N8O2
CrystEngComm (2010) 12, 12 4378
a=10.1652(8)Å b=14.6342(12)Å c=15.2829(12)Å
α=117.5380(10)° β=96.1410(10)° γ=104.3380(10)°
C26H21CuN4O5.5S
C26H21CuN4O5.5S
CrystEngComm (2010) 12, 12 4378
a=18.175(3)Å b=8.7350(15)Å c=30.413(5)Å
α=90.00° β=90.00° γ=90.00°
C9H66Ge2K2Mo16N6O71
C9H66Ge2K2Mo16N6O71
CrystEngComm (2014) 16, 29 6784
a=24.552(5)Å b=17.135(3)Å c=19.302(4)Å
α=90° β=111.10(3)° γ=90°
Ge2H60Mo16Na12O88
Ge2H60Mo16Na12O88
CrystEngComm (2014) 16, 29 6784
a=21.051(4)Å b=15.483(3)Å c=13.472(3)Å
α=90° β=103.62(3)° γ=90°
C20H20FeN8Ni
C20H20FeN8Ni
CrystEngComm (2014) 16, 28 6444
a=11.5168(11)Å b=10.1374(8)Å c=9.6121(9)Å
α=90.00° β=103.266(3)° γ=90.00°
C22.5H30.5Ag2FeN8.5O3
C22.5H30.5Ag2FeN8.5O3
CrystEngComm (2014) 16, 28 6444
a=16.3171(9)Å b=13.8577(5)Å c=14.8466(9)Å
α=90.00° β=111.744(6)° γ=90.00°
C22.5H30.5Ag2FeN8.5O3
C22.5H30.5Ag2FeN8.5O3
CrystEngComm (2014) 16, 28 6444
a=16.622(2)Å b=13.9014(10)Å c=15.434(3)Å
α=90.00° β=112.586(17)° γ=90.00°
C24H32Au2FeN9O2.5
C24H32Au2FeN9O2.5
CrystEngComm (2014) 16, 28 6444
a=16.4515(8)Å b=14.2025(7)Å c=14.2637(7)Å
α=90.00° β=112.0840(10)° γ=90.00°
C24H32Au2FeN9O2.5
C24H32Au2FeN9O2.5
CrystEngComm (2014) 16, 28 6444
a=16.7493(16)Å b=14.8047(14)Å c=14.5137(12)Å
α=90.00° β=113.493(3)° γ=90.00°
C6H66Co5N4O57V11
C6H66Co5N4O57V11
CrystEngComm (2014) 16, 6 1187
a=15.209(3)Å b=14.377(3)Å c=12.810(3)Å
α=90.00° β=91.73(3)° γ=90.00°
C33H48CoN7O17
C33H48CoN7O17
Dalton transactions (Cambridge, England : 2003) (2014) 43, 30 11579-11586
a=16.3575(9)Å b=17.3926(9)Å c=14.9132(8)Å
α=90.00° β=110.956(6)° γ=90.00°
C30H33N7O9
C30H33N7O9
Dalton transactions (Cambridge, England : 2003) (2014) 43, 30 11579-11586
a=5.9605(6)Å b=41.573(5)Å c=12.0127(11)Å
α=90.00° β=102.063(10)° γ=90.00°
C30H36N8O13
C30H36N8O13
Dalton transactions (Cambridge, England : 2003) (2014) 43, 30 11579-11586
a=7.1760(8)Å b=14.1252(14)Å c=17.4500(18)Å
α=108.268(9)° β=91.425(9)° γ=103.228(9)°
C30H36ClN7O14
C30H36ClN7O14
Dalton transactions (Cambridge, England : 2003) (2014) 43, 30 11579-11586
a=7.1623(6)Å b=13.8115(15)Å c=17.8102(13)Å
α=107.186(9)° β=92.852(6)° γ=97.661(8)°
C30H39CoN7O13.5
C30H39CoN7O13.5
Dalton transactions (Cambridge, England : 2003) (2014) 43, 30 11579-11586
a=13.1062(16)Å b=13.1062(16)Å c=35.354(7)Å
α=90.00° β=90.00° γ=120.00°
H122K4Li10Mo2Na24O249P8W48
H122K4Li10Mo2Na24O249P8W48
Dalton transactions (Cambridge, England : 2003) (2012) 41, 38 11700-11705
a=25.7557(17)Å b=25.7557(17)Å c=22.031(2)Å
α=90.00° β=90.00° γ=90.00°
Cu10H144Li16Na12O265P8W48
Cu10H144Li16Na12O265P8W48
Dalton transactions (Cambridge, England : 2003) (2012) 41, 38 11700-11705
a=37.588(8)Å b=25.978(5)Å c=14.420(3)Å
α=90.00° β=98.85(3)° γ=90.00°
C3H54Mn2N7O55PV18
C3H54Mn2N7O55PV18
Dalton transactions (Cambridge, England : 2003) (2015) 44, 47 20435-20440
a=12.1286(19)Å b=20.336(3)Å c=21.324(3)Å
α=90.00° β=90.00° γ=90.00°
H37Mn4O61PV18
H37Mn4O61PV18
Dalton transactions (Cambridge, England : 2003) (2015) 44, 47 20435-20440
a=29.0398(13)Å b=29.0398(13)Å c=24.4712(19)Å
α=90.00° β=90.00° γ=90.00°
C56H56N16NiO42V3W12
C56H56N16NiO42V3W12
Dalton transactions (Cambridge, England : 2003) (2014) 43, 43 16265-16269
a=22.927(5)Å b=22.927(5)Å c=15.430(3)Å
α=90.00° β=90.00° γ=90.00°
Gd12
C132H222Gd12N12O90P12,CoH12O6,18(H2O)4(H16C6N)8(H3C2N)
Dalton transactions (Cambridge, England : 2003) (2016) 45, 22 9041-9044
a=28.0168(10)Å b=28.0168(10)Å c=21.7936(7)Å
α=90° β=90° γ=90°
Bis{1-[bis(2-aminoethyl)amino]propan-2-ol}nickel(II) bis(perchlorate)
C14H38N6NiO22,2(ClO4)
Acta Crystallographica Section E (2007) 63, 11 m2754-m2754
a=7.915(3)Å b=17.243(6)Å c=9.127(3)Å
α=90.00° β=106.442(4)° γ=90.00°
2-[1-(2-Hydroxypropyliminio)ethyl]-5-methoxyphenolate
C12H17NO3
Acta Crystallographica Section E (2006) 62, 12 o5916-o5917
a=5.714(2)Å b=9.672(4)Å c=10.869(3)Å
α=98.19(2)° β=96.71(2)° γ=93.35(3)°
Bis(1<i>H</i>-benzimidazole-κ<i>N</i>^3^)bis[2-(naphthalen-1-yl)acetato- κ^2^<i>O</i>,<i>O</i>]manganese(II) monohydrate
C38H30MnN4O4,H2O
Acta Crystallographica Section E (2012) 68, 3 m328
a=11.654(7)Å b=20.013(12)Å c=14.329(12)Å
α=90.00° β=106.148(7)° γ=90.00°
C24H135Cu6GeN24Nb12O62V2
C24H135Cu6GeN24Nb12O62V2
Crystal Growth & Design (2014) 14, 1 110
a=20.709(4)Å b=20.757(4)Å c=14.872(3)Å
α=90.00° β=129.01(3)° γ=90.00°
C24H138Cu6N24Nb12O63SiV2
C24H138Cu6N24Nb12O63SiV2
Crystal Growth & Design (2014) 14, 1 110
a=20.746(4)Å b=20.789(4)Å c=14.940(3)Å
α=90.00° β=129.11(3)° γ=90.00°
C12H94Cu3GeK2N12Na4Nb12O65V2
C12H94Cu3GeK2N12Na4Nb12O65V2
Crystal Growth & Design (2014) 14, 1 110
a=28.918(6)Å b=27.275(5)Å c=13.638(3)Å
α=90.00° β=93.88(3)° γ=90.00°
C12H86Cu3K2N12Na4Nb12O61SiV2
C12H86Cu3K2N12Na4Nb12O61SiV2
Crystal Growth & Design (2014) 14, 1 110
a=28.942(6)Å b=27.294(6)Å c=13.568(3)Å
α=90.00° β=93.87(3)° γ=90.00°
C25H24O3
C25H24O3
Journal of the American Chemical Society (2020) 142, 21 9763-9771
a=8.9325(2)Å b=10.8470(3)Å c=10.2984(3)Å
α=90° β=96.1030(10)° γ=90°
C23H22BrF3N2O5
C23H22BrF3N2O5
Journal of the American Chemical Society (2018)
a=10.5499(6)Å b=19.6382(11)Å c=11.6438(6)Å
α=90.00° β=96.629(2)° γ=90.00°
C24H24BrClF3NO3
C24H24BrClF3NO3
Journal of the American Chemical Society (2018)
a=11.6781(4)Å b=13.5026(4)Å c=15.2910(5)Å
α=90.00° β=90.00° γ=90.00°
C22H20BrClF3NO3
C22H20BrClF3NO3
Journal of the American Chemical Society (2018)
a=22.803(2)Å b=8.0763(8)Å c=13.3188(14)Å
α=90.00° β=117.960(3)° γ=90.00°
Co16H92Na28O204P8W36
Co16H92Na28O204P8W36
Journal of the American Chemical Society (2014) 136, 14 5359-5366
a=35.8365(17)Å b=35.8365(17)Å c=35.8365(17)Å
α=90.00° β=90.00° γ=90.00°
Co16H116Na32O216P4Si4W36
Co16H116Na32O216P4Si4W36
Journal of the American Chemical Society (2014) 136, 14 5359-5366
a=23.950(3)Å b=23.950(3)Å c=23.950(3)Å
α=90.00° β=90.00° γ=90.00°
Co16H146K2Na30O231P4Si4W36
Co16H146K2Na30O231P4Si4W36
Journal of the American Chemical Society (2014) 136, 14 5359-5366
a=35.6715(17)Å b=35.6715(17)Å c=35.6715(17)Å
α=90.00° β=90.00° γ=90.00°
Co16Ge4H240Na32O278P4W36
Co16Ge4H240Na32O278P4W36
Journal of the American Chemical Society (2014) 136, 14 5359-5366
a=23.924(3)Å b=23.924(3)Å c=23.924(3)Å
α=90.00° β=90.00° γ=90.00°
Co16Ge4H114K2Na30O215P4W36
Co16Ge4H114K2Na30O215P4W36
Journal of the American Chemical Society (2014) 136, 14 5359-5366
a=35.6328(15)Å b=35.6328(15)Å c=35.6328(15)Å
α=90.00° β=90.00° γ=90.00°
As4Co16H120Na28O218P4W36
As4Co16H120Na28O218P4W36
Journal of the American Chemical Society (2014) 136, 14 5359-5366
a=35.514(4)Å b=35.514(4)Å c=35.514(4)Å
α=90.00° β=90.00° γ=90.00°
C26H25Ag3FeN8O2
C26H25Ag3FeN8O2
Inorganic chemistry (2014) 53, 8 4039-4046
a=12.0144(4)Å b=16.9892(6)Å c=31.2716(13)Å
α=90.00° β=90.00° γ=90.00°
C26H25Ag3FeN8O2
C26H25Ag3FeN8O2
Inorganic chemistry (2014) 53, 8 4039-4046
a=12.0015(5)Å b=17.0849(8)Å c=31.3706(16)Å
α=90.00° β=90.00° γ=90.00°
C7H22Cl2ErNO9
C7H22Cl2ErNO9
Dalton transactions (Cambridge, England : 2003) (2013) 42, 36 12853-12856
a=9.0957(2)Å b=15.1667(3)Å c=12.0825(3)Å
α=90.00° β=109.627(2)° γ=90.00°
C22.5H30.5Ag2FeN8.5O3
C22.5H30.5Ag2FeN8.5O3
CrystEngComm (2014) 16, 28 6444
a=16.2400(7)Å b=13.6625(5)Å c=14.8867(7)Å
α=90.00° β=111.728(5)° γ=90.00°
Co16H128Na28O222P8W36
Co16H128Na28O222P8W36
Journal of the American Chemical Society (2014) 136, 14 5359-5366
a=28.666(6)Å b=31.619(6)Å c=26.071(5)Å
α=90.00° β=90.00° γ=90.00°
C26H25Ag3FeN8O2
C26H25Ag3FeN8O2
Inorganic chemistry (2014) 53, 8 4039-4046
a=12.0545(4)Å b=17.2800(6)Å c=31.6186(9)Å
α=90.00° β=90.00° γ=90.00°
C36H24Ag2FeN8
C36H24Ag2FeN8
Inorganic chemistry (2014) 53, 8 4039-4046
a=8.838(2)Å b=16.380(5)Å c=12.421(4)Å
α=90.00° β=108.642(4)° γ=90.00°